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Factory Free sample 1,3-Dihydroxypropane - Dichloroacetyl chloride – MingXing
Factory Free sample 1,3-Dihydroxypropane - Dichloroacetyl chloride – MingXing Detail:
Quality index:
Appearance:Colorless Transparent Liquid
Content: ≥ 99%
Melting point < 25oC
Boiling point: 107-108oC (lit.)
Density: 1.533 g / ml at 20oC
Refractive index N20 / D 1.46 (lit.)
Flash point: 66oC
Instruction:
Used in organic synthesis, pesticide and pharmaceutical intermediates.It is used in the synthesis of vinyl insecticide, wool felting finishing, bleaching, decolorization, preservation, sterilization, disinfection, etc..
Operation precautions: closed operation, pay attention to ventilation. Operators must be specially trained and strictly abide by the operating procedures. It is recommended that operators wear self-priming filter gas mask (full mask), rubber acid and alkali resistant clothing and rubber acid and alkali resistant gloves. Keep away from fire and heat source. No smoking in the workplace. Use explosion-proof ventilation system and equipment. Avoid smoke. Prevent the release of smoke and steam into the workplace air. Avoid contact with oxidant, alkali and alcohol. In particular, avoid contact with water. When carrying, it should be loaded and unloaded lightly to prevent the package and container from being damaged. Fire fighting equipment of corresponding variety and quantity and leakage emergency treatment equipment shall be provided. Empty containers may contain harmful substances.
Storage precautions: store in a cool, dry and well ventilated warehouse. Keep away from fire and heat source. Keep the container sealed. It should be stored separately from oxidants, alkalis and alcohols, and mixed storage should be avoided. Fire fighting equipment of corresponding variety and quantity shall be provided. The storage area shall be equipped with leakage emergency treatment equipment and suitable storage materials.
Production method: various process routes can be used in the preparation method. The product can be prepared by the reaction of dichloroacetic acid with chlorosulfonic acid, the reaction of chloroform with carbon monoxide catalyzed by anhydrous aluminum trichloride, the reaction of dichloroacetic acid with phosgene in dimethylformamide, and the oxidation of trichloroethylene. Trichloroethylene and azodiisobutyronitrile (catalyst) were heated to 100 ℃, oxygen was introduced, and the reaction was carried out under the pressure of 0.6MPa. The oil bath temperature was maintained at 110 ℃ for 10h, and dichloroacetyl chloride was evaporated under normal pressure. The by-product trichloroethylene oxide can also be converted into dichloroacetyl chloride by the reaction with methylamine, triethylamine, pyridine and other amines.
Packing: 250kg / drum.
Annual capacity: 3000 tons / year
Product detail pictures:
Related Product Guide:
Our concentrate on should be to consolidate and enhance the quality and service of present products, meanwhile consistently produce new products to meet unique customers' demands for Factory Free sample 1,3-Dihydroxypropane - Dichloroacetyl chloride – MingXing , The product will supply to all over the world, such as: Sweden, Estonia, Jamaica, They're durable modeling and promoting well all over the world. Under no circumstances disappearing key functions in a brief time, it's a should for you personally of fantastic quality. Guided by the principle of Prudence, Efficiency, Union and Innovation. the business make an awesome efforts to expand its international trade, raise its enterprise. rofit and improve its export scale. We are confident that we'll have a vibrant prospect and to be distributed all over the world in the years to come.
By Edith from Muscat - 2017.10.27 12:12
We are long-term partners, there is no disappointment every time, we hope to maintain this friendship later!
By Bess from Burundi - 2017.06.22 12:49
